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ARS Home » Northeast Area » Beltsville, Maryland (BHNRC) » Beltsville Human Nutrition Research Center » Methods and Application of Food Composition Laboratory » Research » Research Project #436105

Research Project: Advanced Technology for Rapid Comprehensive Analysis of the Chemical Components

Location: Methods and Application of Food Composition Laboratory

Publications (Clicking on the reprint icon Reprint Icon will take you to the publication reprint.)

Comprehensive oligosaccharide profiling of commercial almond milk, soy milk, and soy flour Reprint Icon - (Peer Reviewed Journal)
Huang, Y., Bruna, P., Fukagawa, N.K., Barile, D. 2022. Comprehensive oligosaccharide profiling of commercial almond milk, soy milk, and soy flour. Food Chemistry. 409:135267. https://doi.org/10.1016/j.foodchem.2022.135267.

Quantitative bottom-up glycomic analysis of polysaccharides in food matrices using liquid chromatography – tandem mass spectrometry Reprint Icon - (Peer Reviewed Journal)
Bacalzo, N., Couture, G., Ye, C., Castillo, J., Phillips, K., Fukagawa, N.K., Lebrilla, C. 2022. Quantitative bottom-up glycomic analysis of polysaccharides in food matrices using liquid chromatography – tandem mass spectrometry. Analytical Chemistry. 95:1008. https://doi.org/10.1021/acs.analchem.2c03707.

Oxidative Stress and Antioxidants - A Critical Review on in-vitro Antioxidant Assays Reprint Icon - (Literature Review)
Kotha, R.R., Tareq, F.S., Yildiz, E., Luthria, D.L. 2022. Oxidative Stress and Antioxidants - A Critical Review on in-vitro Antioxidant Assays. Molecules. 11:2388. https://doi.org/10.3390/antiox11122388.

Three-dimensional liquid chromatography with parallel second dimensions and quadruple parallel mass spectrometry for infant formula Reprint Icon - (Peer Reviewed Journal)
Byrdwell, W.C., Hari, K.K., Goldschmidt, R.J., Jakubec, P., Novakova, L. 2022. Three-dimensional liquid chromatography with parallel second dimensions and quadruple parallel mass spectrometry for infant formula. Journal of Chromatography. 1661:462682. https://doi.org/10.1016/j.chroma.2021.462682.

Multi-glycomic characterization of fiber from AOAC methods defines the carbohydrate structures Reprint Icon - (Peer Reviewed Journal)
Bacalzo,.P., Couture, G., Ye, C., Luthria, D.L., Phillips, K.M., Fukagawa, N.K., Lebrilla, C.B., Tareq, F.S., Harnly, J.M., Pehrsson, P.R., McKillop, K.A. 2022. Multi-glycomic characterization of fiber from AOAC methods defines the carbohydrate structures. Journal of Agricultural and Food Chemistry. 70(45):14559-14570. https://doi.org/10.1021/acs.jafc.2c06191.

Extractability of Curcuminoids is Enhanced with Milk and Aqueous-Alcohol Mixtures Reprint Icon - (Peer Reviewed Journal)
Kotha, R.R., Tareq, F.S., Luthria, D.L. 2022. Extractability of Curcuminoids is Enhanced with Milk and Aqueous-Alcohol Mixtures. ACS Food Science and Technology. 27:4883. https://doi.org/10.3390/molecules27154883.

Mass Spectrometry Based Non-Targeted and Targeted Analytical Approaches in Fingerprinting and Metabolomics of Food and Agricultral Research Reprint Icon - (Review Article)
Zhihao, L., Mengliang, Z., Chen, P., Harnly, J.M., Sun, J. 2022. Mass spectrometry based non-targeted and targeted analytical approaches in fingerprinting and metabolomics of food and agricultral research. Journal of Agriculture and Food Chemistry. 70(36):11138–11153. https://doi.org/10.1021/acs.jafc.2c01878.

Deep learning accurately predicts food categories and nutrients based on ingredient statements Reprint Icon - (Peer Reviewed Journal)
Ma, P., Wang, Q., Yu, N., Li, Y., Zhang, Z., Sheng, J., Ahuja, J.K., Mcginty, H. 2022. Deep learning accurately predicts food categories and nutrients based on ingredient statements. Food Chemistry. 391:133243. https://doi.org/10.1016/j.foodchem.2022.133243.

Contrast study on secondary metabolite profile between pastas made from three single varietal common bean (Phaseolus vulgaris L.) and durum wheat (Triticum durum) Reprint Icon - (Peer Reviewed Journal)
Geng, P., Hooper, S., Sun, J., Chen, P., Cichy, K.A., Harnly, J.M. 2022. Contrast study on secondary metabolite profile between pastas made from three single varietal common bean (Phaseolus vulgaris L.) and durum wheat (Triticum durum). ACS Food Science and Technology. 2(5):895–904. https://doi.org/10.1021/acsfoodscitech.2c00050.

Profiling of polyphenols and glucosinolates in kale and broccoli microgreens grown under chamber and windowsill conditions by ultrahigh-performance liquid chromatography high-resolution mass spectrometry Reprint Icon - (Peer Reviewed Journal)
Liu, Z., Shi, J., Wan, J., Pham, Q., Zhang, Z., Sun, J., Yu, L., Luo, Y., Wang, T.T.Y., Chen, P. 2021. Profiling of polyphenols and glucosinolates in kale and broccoli microgreens grown under chamber and windowsill conditions by ultrahigh-performance liquid chromatography high-resolution mass spectrometry. ACS Food Science and Technology. 2(1):101-113. https://doi.org/10.1021/acsfoodscitech.1c00355.

Deriving Information from Complex Data Sets: Impact of Forage on Fatty Acids in Cow Milk Reprint Icon - (Peer Reviewed Journal)
Harnly, J.M., Picklo, M., Bukowski, M.R., Kalscheur, K., Magnuson, A.D., Fukagawa, N.K., Finley, J.W. 2021. Deriving information from complex data sets: Impact of forage on fatty acids in cow milk. Journal of Food Composition and Analysis. 107:104179. https://doi.org/10.1016/j.jfca.2021.104179.

Identification of marker compounds for predicting browning of fresh-cut lettuce using untargeted UHPLC-HRMS metabolomics Reprint Icon - (Peer Reviewed Journal)
Liu, Z., Sun, J., Teng, Z., Luo, Y., Yu, L., Simko, I., Chen, P. 2021. Identification of marker compounds for predicting browning of fresh-cut lettuce using untargeted UHPLC-HRMS metabolomics. Postharvest Biology and Technology. 180.Article 111626. https://doi.org/10.1016/j.postharvbio.2021.111626.

GC-MS and GC-FID of seven seed oils containing conjugated fatty acids Reprint Icon - (Peer Reviewed Journal)
Goldschmidt, R.J., Byrdwell, W.C. 2021. GC-MS and GC-FID of seven seed oils containing conjugated fatty acids. Journal of Chromatographic Science. 43:259–273.. https://doi.org/10.3390/separations8040051.

Two- and three-dimensional chromatography with four dimensions of mass spectrometry, LC2MS4 and LC3MS4: Breaking the rules - (Peer Reviewed Journal)
Byrdwell, W.C. 2021. Two- and three-dimensional chromatography with four dimensions of mass spectrometry, LC2MS4 and LC3MS4: Breaking the rules. Current Trends in Mass Spectrometry. 49: 446–457.

Influence of moderate-to-high salinity on the phytochemical profile of two salinity-tolerant spinach genotypes Reprint Icon - (Peer Reviewed Journal)
Tareq, F.S., Kotha, R.R., Ferreira, J.F., Sandhu, D., Luthria, D.L. 2021. Influence of moderate-to-high salinity on the phytochemical profile of two salinity-tolerant spinach genotypes. ACS Food Science and Technology. 1 205–214. https://doi.org/10.1021/acsfoodscitech.0c00034.

Changes in Compositions of Galactolipids, Triacylglycerols, and Tocopherols of Lettuce Varieties (Lactuca sativa L.) with Type, Age, and Light Source Reprint Icon - (Peer Reviewed Journal)
Byrdwell, W.C., Kubzdela, ., Goldschmidt, R.J. 2020. Changes in Compositions of Galactolipids, Triacylglycerols, and Tocopherols of Lettuce Varieties (Lactuca sativa L.) with Type, Age, and Light Source. Journal of Agricultural and Food Chemistry. 4:242-248. https://doi.org/10.1016/j.jfca.2020.103631.

Comparison of Phytochemical Composition of Ginkgo biloba Extracts Using a Combination of Non-targeted and Targeted Analytical Approaches Reprint Icon - (Peer Reviewed Journal)
Collins, B., Rider, C., Waidyanatha, ., Mueller, G., Derose, E., London, R., Kerns, S., Aillon,, K., Harnly, J.M. 2020. Comparison of Phytochemical Composition of Ginkgo biloba Extracts Using a Combination of Non-targeted and Targeted Analytical Approaches. Analytical and Bioanalytical Chemistry. 412:6789–6809. https://doi.org/10.1007/s00216-020-02839-7.

A systematic approach to determine the impact of elevated CO2 levels on the chemical composition of wheat (Triticum aestivum) Reprint Icon - (Peer Reviewed Journal)
Geng, P., Sun, J., Chen, P., Li, Y., Peng, B., Harnly, J.M. 2020. A systematic approach to determine the impact of elevated CO2 levels on the chemical composition of wheat (Triticum aestivum). Journal of Cereal Science. 95:753. https://doi.org/10.1016/j.jcs.2020.103020.

Identification of Adulteration in Botanical Samples Supplements with Untargeted Metabolomics Reprint Icon - (Peer Reviewed Journal)
Kellogg, J.J., Wallace, E.D., Todd, D.A., Cech, N.B., Harnly, J.M. 2020. Identification of Adulteration in Botanical Samples Supplements with Untargeted Metabolomics. Analytical and Bioanalytical Chemistry. 41: 4273-4286. https://doi.org/10.1007/s00216-020-02678-6.

Characterization of Maca (Lepidium meyenii/Lepidium peruvianum) Using a Mass Spectral Fingerprinting, Metabolomic Analysis, and Genetic Sequencing Approach Reprint Icon - (Peer Reviewed Journal)
Geng, P., Sun, J., Brand, E., Frame, J., Meissner, H., Stewart, J., Clark, S., Miller, J., Harnly, J.M., Chen, P., Gafner, S. 2020. Characterization of Maca (Lepidium meyenii/Lepidium peruvianum) using a mass spectral fingerprinting, metabolomic analysis, and genetic sequencing approach. Planta Medica. 169:453–468. https://doi.org/10.1055/a-1161-0372.

Analysis of Cranberry Proanthocyanidins Using UPLC - Ion Mobility - High Resolution Mass Spectrometry Reprint Icon - (Peer Reviewed Journal)
Wang, Y., Harrington, P.B., Chang, T., Wu, X., Chen, P. 2020. Analysis of cranberry proanthocyanidins using UPLC - ion mobility - high resolution mass spectrometry. Analytical and Bioanalytical Chemistry. 412:3653-3662. https://doi.org/10.1007/s00216-020-02601-z.

Improving Natural Product Research Translation: from Source to Clinical Trial - (Peer Reviewed Journal)

Terms and momenclature used for plant-derived components in nutrition and related research: Efforts toward harmonization - (Peer Reviewed Journal)

Chemical profile and in vitro gut microbiota modulatory, anti-inflammatory and free radical scavenging Properties of chrysanthemum morifolium cv. Fubaiju Reprint Icon - (Peer Reviewed Journal)
Li, Y., Hao, Y., Gao, B., Geng, P., Huang, H., Yu, L., Choe, U., Liu, J., Sun, J., Chen, P., Wang, T.T.Y., Yu, L. 2019. Chemical profile and in vitro gut microbiota modulatory, anti-inflammatory and free radical scavenging properties of chrysanthemum morifolium cv. Fubaiju. Journal of Functional Foods. 58:114-122. https://doi.org/10.1016/j.jff.2019.04.053.

Curcumin: Pharmaceutical, Nutraceutical, and Analytical Aspects Reprint Icon - (Review Article)

Non-targeted detection of milk powder adulteration by 1H NMR spectroscopy and Conformity Index Analysis Reprint Icon - (Peer Reviewed Journal)
Bergana, M., Adams, K., Harnly, J.M., Moore, J., Xie, Z. 2020. Non-targeted detection of milk powder adulteration by 1H NMR spectroscopy and conformity index analysis. Journal of Food Composition and Analysis. https://doi.org/10.1016/j.jfca.2019.01.016.