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United States Department of Agriculture

Agricultural Research Service

Title: Threshold Values for Key Aroma Components in An Orange Juice Matrix: Esters

Authors
item Plotto, Anne
item Margaria, Carlos - UNITED STATES DISTILLED
item Goodner, Kevin
item Baldwin, Elizabeth

Submitted to: Annual Meeting of the Institute of Food Technologists
Publication Type: Abstract Only
Publication Acceptance Date: December 20, 2003
Publication Date: July 1, 2004
Citation: Plotto, A., Margaria, C.A., Goodner, K.L., Baldwin, E.A. 2004. Threshold values for key aroma components in an orange juice matrix: esters. Annual Meeting of the Institute of Food Technologists. p. 70. Paper No. 33B-5.

Technical Abstract: Thresholds for flavor volatiles have been traditionally calculated in water or air, but they may vary widely in more complex matrices such as milk, gels, or fruit slurries. The data presented is part of a continuing study to provide the industry with threshold guidelines more adequate for the use of flavors in citrus juices. The objectives include understanding of volatile-matrix interactions. Thresholds of key aroma compounds of orange juice (OJ) were determined in a deodorized OJ matrix. The Three-Alternative-Forced-Choice (3-AFC) method was used (ASTM: E-679). Sixteen to twenty experienced panelists were presented with orange juice samples arranged in five rows of three samples corresponding to five spiking levels, each separated by a factor of 3, with a 3-AFC presentation at each level. For each compound, the test was repeated four times. Compounds tested were verified for purity by GC/MS and GC/O. Odor and taste thresholds for esters were twice (methyl butanoate) to thirty times (ethyl propanoate) higher in the orange juice matrix than published values in water. In comparison, it was found earlier that for non-water soluble compounds, odor thresholds in the juice were over 200 times higher than in water (a- and ß-pinene, octanal, limonene), while for more soluble aldehydes and the terpene-alcohol linalool, the threshold in juice was about 10 times higher than published values in water. Odor thresholds were generally higher than taste thresholds. For some compounds, perception of the sweet taste in the blank was decreased when compounds were at levels below the recognition threshold. These results show the importance non-soluble compounds on odor and flavor perception. The effect of compound purity and pulp level in the juice will be discussed. The threshold values provided by this research is directly applicable by the industry in comparison with the current values that are published in water.

Last Modified: 7/24/2014
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