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United States Department of Agriculture

Agricultural Research Service

Research Project: THE ADVANCEMENT OF SPECTROSCOPIC SENSORS/CHEMOMETRIC ANALYSIS/BIOBASED PRODUCTS FOR QUALITY ASSESSMENT OF FIBER, GRAIN, AND FOOD COMMODITIES

Location: Quality and Safety Assessment Research Unit

Title: Dielectric Study of Binding Modes of Water in Grain and Seed at Low Temperatures

Authors
item Trabelsi, Samir
item Nelson, Stuart

Submitted to: Microwave Power Symposium Proceedings
Publication Type: Proceedings
Publication Acceptance Date: May 30, 2006
Publication Date: August 9, 2006
Citation: Trabelsi, S., Nelson, S.O. 2006. Dielectric study of binding modes of water in grain and seed at low temperatures. 40th Annual Microwave Symposium Proceedings. August 9-11, 2006, Boston, MA. pp.89-92.

Interpretive Summary: The moisture content of cereal grains is very important in determining how long such commodities can be safely stored without spoilage and loss of value. Electrical moisture meters determine grain and seed moisture content by sensing their electrical characteristics, called dielectric properties, which are closely correlated with moisture content. There is need to improve the accuracy of moisture meters, and measurements at microwave frequencies, much higher than the frequencies used by current moisture meters, offer some advantages. Therefore, the way in which the dielectric properties depend on the water in the grain and seed is important. The research reported was carried out to gain new knowledge about the nature of bound water held in grain. The aim was to obtain a better understanding of the way microwave dielectric properties of grain change with temperature, and by studying this behavior at very low temperatures, minus 70 degrees to plus 21 degrees C, new information was obtained on the dielectric behavior of bound water. A change in slope of the line representing dielectric properties at different temperatures revealed that bound water is most likely frozen at about minus 20 degrees C, whereas liquid water freezes at about 0 degrees C. With better understanding of the dielectric behavior of water in grain, the accuracy of rapid sensing of moisture content by microwave moisture meters can be improved. Better moisture sensing can be achieved to preserve quality of grain and seed and provide higher quality products for consumers.

Technical Abstract: Dielectric behavior of bound water in grain and seed was investigated through measurement of the dielectric properties at microwave frequencies over a wide temperature range between minus 70 degrees C and +21 degrees C. Samples of wheat and soybeans were cooled to minus 70 degrees C and then their dielectric properties were tracked with a free-space transmission measurement system between 2 and 18 GHz while they warmed up to room temperature. Results showed that both the dielectric constant, epsilon prime, and loss factor, epsilon double prime, increased with temperature with a characteristic slope change and a higher increase rate at around minus 20 degrees C.

Last Modified: 7/30/2014
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