Projects

PATTERN RECOGNITION FOR FOODS AND SUPPLEMENTS General Cooperative Agreement (A)   Accession Number: 414639

MEASUREMENT SYSTEMS FOR DETERMINATION OF VITAMINS IN FOODS AND DIETARY SUPPLEMENTS Appropriated (D)   Accession Number: 416459

FINGERPRINTING AND PROFILING METHODS FOR CHARACTERIZATION OF FOODS AND DIETARY SUPPLEMENTS Appropriated (D)   Accession Number: 416462

DEVELOPMENT OF SPECTRAL FINGERPRINTING METHODS FOR RAPID CHARACTERIZATION AND AUTHENTICATION OF BOTANICAL DIETARY SUPPLEMENTS Reimbursable (R)   Accession Number: 419644

USE OF INFORMATION TECHNOLOGIES FOR DIETARY COMPOSITION AND SURVEY EVALUATIONS Specific Cooperative Agreement (S)   Accession Number: 422998

DNA BARCODES/FINGERPRINTS, CHEMICAL FINGERPRINTS, AND METABOLOMIC PROFILES FOR BOTANICAL SUPPLEMENTS Specific Cooperative Agreement (S)   Accession Number: 423521

METABOLOMIC METHODS FOR PLANT AND ANIMAL SPECIMENS Specific Cooperative Agreement (S)   Accession Number: 423531

Publications (Clicking on the reprint icon will take you to the publication reprint.)

Classification of cultivation locations of panax quinquefolius L samples using high performance liquid chromatography-electrospray ionization mass spectrometry and chemometric analysis - (Peer Reviewed Journal)

Sun, X., Chen, P., Cook, S., Jackson, G., Harnly, J.M., Harrington, P. 2012. Classification of cultivation locations of panax quinquefolius L samples using high performance liquid chromatography-electrospray ionization mass spectrometry and chemometric analysis. Analytical Chemist. 84:3628-3634.

LC-PDA-ESI/MS Identification of the Phenolic Components of Three Compositae Spices: Chamomile, Tarragon, and Mexican Arnica - (Peer Reviewed Journal)

Lin, L., Harnly, J.M. 2012. LC-PDA-ESI/MS Identification of the Phenolic Components of Three Compositae Spices: Chamomile, Tarragon, and Mexican Arnica. Natural Product Communications. 7:749-753.

A general approach to quantification of hydroxycinnamic acid derivatives and flavones, flavonols, and their glycosides by UV spectrophotometry - (Peer Reviewed Journal)

Lin, L., Harnly, J.M., Zhang, R., Chen, H., Fain, Z. 2011. A general approach to quantification of hydroxycinnamic acid derivatives and flavones, flavonols, and their glycosides by UV spectrophotometry. Journal of Agricultural and Food Chemistry. 60:544-553.

UHPLC-PDA-ESI/HRMS/MSn analysis of anthocyanins, flavonol glycosides, and hydroxycinnamic acid derivatives in red mustard green (Brassica juncea (L) Coss variety) - (Peer Reviewed Journal)

Lin, L., Sun, J., Chen, P., Harnly, J.M. 2011. UHPLC-PDA-ESI/HRMS/MSn analysis of anthocyanins, flavonol glycosides, and hydroxycinnamic acid derivatives in red mustard green (Brassica juncea (L) Coss variety). Journal of Agricultural and Food Chemistry. 60:544-553.

Guidelines for validation of botanical identification methods - (Peer Reviewed Journal)

Harnly, J.M., Applequist, W., Caspar, S., Harrington, P., Hill, N., Labudde, R., Neal-Kababick, J., Harbaugh-Reynaud, D., Roman, M., Roman, S., Sullivan, D., Titlow, B., Wehling, P. 2012. Guidelines for validation of botanical identification methods. Official Methods of Analysis of AOAC International. 95:268-272.

Probability of identification (POI): a statistical model for the validation of qualitative botanical identification methods - (Peer Reviewed Journal)

Labudde, R., Harnly, J.M. 2012. Probability of identification (POI): a statistical model for the validation of qualitative botanical identification methods. Official Methods of Analysis of AOAC International. 95:273-285.

Quantitation of flavanols, proanthocyanidins, isoflavones, flavanones, dihydrochalcones, stilbenes, and benzoic Acid derivatives after identification by LC-MS - (Peer Reviewed Journal)

Lin, L., Harnly, J.M. 2011. Quantitation of flavanols, proanthocyanidins, isoflavones, flavanones, dihydrochalcones, stilbenes, and benzoic Acid derivatives after identification by LC-MS. Journal of Agricultural and Food Chemistry. 60:5832-5840.

LC-PDA-EIS/MSn identification of new anthocyanins in purple radish (Raphanus sativus L. variety) - (Peer Reviewed Journal)

Lin, L., Jianghao, S., Chen, P., Harnly, J.M. 2011. LC-PDA-EIS/MSn identification of new anthocyanins in purple radish (Raphanus sativus L. variety). Journal of Agricultural food Chemistry . 59:6616-6627.

A statistical evaluation of spectral fingerprinting methods using analysis of variance and principal component analysis - (Peer Reviewed Journal)

Luthria, D.L., Mukhopadhyay, S., Lin, L., Harnly, J.M. 2011. A statistical evaluation of spectral fingerprinting methods using analysis of variance and principal component analysis. Food Chemistry. 65:80-85.

Identification, quantitation, and comprehensive assessment of green, white, and pu-erh teas using UPLC/UV/MS - (Peer Reviewed Journal)

Zhao, Y., Chen, P., Lin, L., Harnly, J.M. 2011. Identification, quantitation, and comprehensive assessment of green, white, and pu-erh teas using UPLC/UV/MS. Food Chemistry. 126:1269-1277.

Discrimination among Panax species using spectral fingerprinting - (Peer Reviewed Journal)

Chen, P., Luthria, D.L., Harrington, P.B., Harnly, J.M. 2011. Discrimination among Panax species using spectral fingerprinting. Journal of the Association of Official Analytical Chemists. 94:1411-1421.

A non-targeted approach to chemical discrimination between green tea extract-based dietary supplements and green tea leaves by LC/MS - (Peer Reviewed Journal)

Sun, J., Chen, P., Lin, L., Harnly, J.M. 2011. A non-targeted approach to chemical discrimination between green tea extract-based dietary supplements and green tea leaves by LC/MS. Journal of the Association of Official Analytical Chemists. 94:487-497.

Ultraviolet and mass spectrometric analysis of vitamin D in retail fortified orange juice - (Peer Reviewed Journal)

Byrdwell, W.C., Exler, J., Gebhardt, S.E., Harnly, J.M., Holden, J.M., Horst, R., Patterson, K.K., Phillips, K., Wolf, W.R. 2010. Ultraviolet and mass spectrometric analysis of vitamin D in retail fortified orange juice. Journal of Food Composition and Analysis. 24:299-306.

Phenolic component profiles of mustard greens, yu choy and 15 other Brassica vegatables - (Peer Reviewed Journal)

Harnly, J.M., Lin, L. 2010. Phenolic component profiles of mustard greens, yu choy and 15 other Brassica vegatables. Journal of Agricultural and Food Chemistry. 58(11):6850-6857.

Flow injection mass spectral fingerprints demonstrate chemical differences in rio red grapefruit with respect to year, harvest time, and conventional versus organic farming - (Peer Reviewed Journal)

Chen, P., Harnly, J.M., Lester, G.E. 2010. Flow injection mass spectral fingerprints demonstrate chemical differences in Rio Red grapefruit with respect to year, harvest time, and conventional versus organic farming. Journal of Agriculture and Food Chemistry. 58(8):4545-4553.

Mass spectroscopic fingerprinting method for to differentiation between Scutellaria lateriflora and the Germander (Teucrium canadens and T. chamaedrys species - (Peer Reviewed Journal)

Chen, P., Lin, L., Harnly, J.M. 2010. Mass spectroscopic fingerprinting method for differentiation between Scutellaria lateriflora and the Germander (Teucrium canadense and T. chamaedrys) species. Journal of AOAC International. 93(4):1148-1154.

Identification of phenolic components of chrysanthemum flower (Chrysanthemum morifolium) - (Peer Reviewed Journal)

Lin, L., Harnly, J.M. 2010. Identification of phenolic components of chrysanthemum flower (Chrysanthemum morifolium Ramat). Food Chemistry 120(1):319-326.

Identification of the phenolic components of collard greens, kale, and Chinese broccoli - (Peer Reviewed Journal)

Lin, L., Harnly, J.M. 2009. Identification of the phenolic components of collard greens, kale, and Chinese broccoli. Journal of Agricultural and Food Chemistry. 57(16):7401-7408.

Legacy of Wilbur O. Atwater: Human Nutrition Research Expansion at the USDA-Interagency Development of Food Composition Research - (Peer Reviewed Journal)

Beecher, G., Stewart, K., Holden, J.M., Harnly, J.M., Wolf, W.R. 2009. Legacy of Wilbur O. Atwater: human nutrition research expansion at the USDA-interagency development of food composition research. Journal of Nutrition. 139:178-184.

Variance in the chemical composition of dry beans determined from UV spectral fingerprints - (Peer Reviewed Journal)

Harnly, J.M., Pastor Corrales, M.A., Luthria, D.L. 2009. Variance in the chemical composition of dry beans determined from UV spectral fingerprints. Journal of Agricultural and Food Chemistry. 57(19):8705-8710.

Optimization of Methodology for Vitamin D3 in Fortified Foods - (Abstract Only)

Patterson, K.K., Exler, J., Lemar, L.E., Holden, J.M., Phillips, K., Harnly, J.M., Byrdwell, W.C., Wolf, W.R. 2008. Optimization of Methodology for Vitamin D3 in Fortified Foods. National Institutes of Health (NIH) Office of Dietary Supplements (ODS) Analytical Methods and Reference Materials Program, Vitamin Methodology Workshop, July 7-8, 2008, Gaithersburg, MD.

Chromatographic profiles of Ginkgo biloba leaves and selected products - (Peer Reviewed Journal)

Lin, L., Chen, P., Ozcan, M., Harnly, J.M. 2008. Chromatographic profiles of Ginkgo biloba leaves and selected products. Journal of Agricultural and Food Chemistry. http://dx.doi.org/10.1021/jf800488x.

UV Spectral Fringerprinting and Analysis of Variance-Principal Component Analysis: A Tool for Characterizing Sources of Variance in Plant Materials - (Peer Reviewed Journal)

Luthria, D.L., Mukhopadhyay, M., Finley, J., Banuelos, G.S., Harnly, J.M. 2008. UV spectral fringerprinting and analysis of variance-principal component analysis: a tool for characterizing sources of variance in plant materials. Journal of Agricultural and Food Chemistry. http://dx.doi.org/10.10.21/jf0734572.

Evaluation and harmonization of measurements of vitamin D in selected food materials - (Peer Reviewed Journal)

Phillips, K., Byrdwell, W.C., Exler, J., Harnly, J.M., Holden, J.M., Holick, M., Hollis, B., Horst, R., Lemar, L.E., Patterson, K.K., Tarrango-Trani, M., Wolf, W.R. 2008. Evaluation and harmonization of measurements of vitamin D in selected food materials. Journal of Food Composition and Analysis. 21:527-534.

A systematic approach to the identification of common hydroxycinnamoylquinic acids in plant materials - (Peer Reviewed Journal)

Lin, L., Harnly, J.M. 2008. A systematic approach to the identification of common hydroxycinnamoylquinic acids in plant materials. Journal of Agricultural and Food Chemistry. 56:10105-10114.

Phenolic compounds and chromatographic profiles of pear skins (Pyrus spp.) - (Peer Reviewed Journal)

Lin, L., Harnly, J.M. 2008. Phenolic compounds and chromatographic profiles of pear skins (Pyrus spp.). Journal of Agricultural and Food Chemistry. 56(19):9094-9101.

New phenolic components and chromatographic profiles of green and fermented teas - (Peer Reviewed Journal)

Lin, L., Harnly, J.M. 2008. New phenolic components and chromatographic profiles of green and fermented teas. Journal of Agricultural and Food Chemistry. 56(17):8130-8140.

Ultraviolet spectral fingerprints: A simple approach for classification of bean cultivars - (Trade Journal)

Luthria, D.L., Pastor Corrales, M.A., Harnly, J.M. 2008. Ultraviolet spectral fingerprints: A simple approach for classification of bean cultivars. Bean Improvement Cooperative Annual Report. 51:132-133.

Analyzing vitamin D in foods and supplements: methodological challenges - (Peer Reviewed Journal)

Byrdwell, W.C., Devries, J., Exler, J., Harnly, J.M., Holden, J.M., Holick, M., Hollis, B., Horst, R., Lada, M., Lemar, L.E., Patterson, K.K., Phillips, K., Tarrago-Trani, M., Wolf, W.R. 2008. Analyzing vitamin D in foods and supplements: Methodological challenges. American Journal of Clinical Nutrition. 88:554S-557S.

Discriminating between cultivars and treatments of broccoli using mass spectral fingerprinting and analysis of variance-principal component analysis - (Peer Reviewed Journal)

Luthria, D.L., Lin, L., Robbins, R.J., Finley, J.W., Banuelos, G.S., Harnly, J.M. 2008. Discriminating between cultivars and treatments of broccoli using mass spectral fingerprinting and analysis of variance-principal component analysis. Journal of Agricultural and Food Chemistry. 56(21):8130-8140.

Comparison of the phenolic component profiles of skullcap (Scutellaria lateriflora) and germander (Teucrium canadense and T. chamaedrys), a potentially hepatotoxic adulterant - (Peer Reviewed Journal)

Lin, L., Harnly, J.M., Upton, R. 2009. Comparison of the phenolic component profiles of skullcap (Scutellaria lateriflora) and germander (Teucrium canadense and T. chamaedrys), a potentially hepatotoxic adulterant. Phytochemical Analysis. 20(4):298-306.

The Polyphenolic Profiles of Common Bean (Phaseolus vulgaris L.) - (Peer Reviewed Journal)

Lin, L., Harnly, J.M., Pastor Corrales, M.A., Luthria, D.L. 2008. The polyphenolic profiles of common bean (Phaseolus vulgaris L.). Journal of Food Chemistry. 107:399-410.

A profiling method for the identification of glycosylated flavonoids and other phenolic compounds using a standard analytical approach for all plant materials - (Abstract Only)

Harnly, J.M., Lin, L. 2008. A profiling method for the identification of glycosylated flavonoids and other phenolic compounds using a standard analytical approach for all plant materials. National Nutrient Databank Conference, May 12-14, 2008, Ottawa, Ontario, Canada, and 5th Annual Natural Health Product Research Society of Canada (NHPRS) Conference, March 26-29, 2008, Toronto, Canada.

Spectral and chromatographic fingerprinting with analysis of variance-principal component analysis (ANOVA-PCA): a useful tool for differentiating botanicals and characterizing sources of variance - (Abstract Only)

Harnly, J.M., Luthria, D.L. 2008. Spectral and chromatographic fingerprinting with analysis of variance-principal component analysis (ANOVA-PCA): a useful tool for differentiating botanicals and characterizing sources of variance. National Nutrient Databank Conference, May 12-14, 2008, Ottawa, Ontario, Canada.

Spectral and chromatographic fingerprinting with analysis of variance-principal component analysis (ANOVA-PCA): a useful tool for differentiating botanicals and characterizing sources of variance - (Abstract Only)

Harnly, J.M., Luthria, D.L. 2008. Spectral and chromatographic fingerprinting with analysis of variance-principal component analysis (ANOVA-PCA): a useful tool for differentiating botanicals and characterizing sources of variance.Natural Health Product Research Society of Canada (NHPRS), March 26-29, 2008, Toronto, Canada.

U.S. Dietary Supplement Ingredient Database (DSID): Adult Multivitamin/Mineral (MVM) Study Results and Implementation Strategies for the First Data Release - (Abstract Only)

Roseland, J.M., Andrews, K., Zhao, C., Holden, J.M., Schweitzer, A., Douglass, L., Harnly, J.M., Wolf, W.R., Dwyer, J., Picciano, M., Saldanha, L., Yetley, E., Fisher, K. 2008. U.S. Dietary Supplement Ingredient Database (DSID): Adult Multivitamin/Mineral (MVM) study results and implementation strategies for the first data release. 32nd National Nutrient Databank Conference, May 12-14, 2008, Ottawa, Ontario, Canada.

Spectral Fingerprinting and Analysis of Variance-Principal Component Analysis: A Tool for Classifying Variance in Plant Materials - (Abstract Only)

Luthria, D.L., Harnly, J.M. 2008. Spectral Fingerprinting and Analysis of Variance-Principal Component Analysis: A Tool for Classifying Variance in Plant Materials. XXIV International Conference on Polyphenols, July 8-11, 2008, Salamanca, Spain.

Variability in the Vitamin D Content of 2% Milk from a Nationwide United States Department of Agriculture (USDA) Sampling - (Abstract Only)

Patterson, K.K., Phillips, K., Horst, R., Byrdwell, W.C., Exler, J., Harnly, J.M., Lemar, L.E., Pehrsson, P.R., Wolf, W.R. 2008. Variability in the vitamin D content of 2% milk from a nationwide United States Department of Agriculture (USDA) sampling. 32nd National Nutrient Databank Conference, May 12-14, 2008, Ottawa, Ontario, Canada.

LC-MS profiling and quantification of food phenolic components using a standard analytical approach for all plants - (Book / Chapter)

Lin, L., Harnly, J.M. 2008. LC-MS profiling and quantification of food phenolic components using a standard analytical approach for all plants. In: Greco, L.V., Bruno, M.N., editors. Food Science and Technology: New Research. New York, NY: Nova Science Publishers, Inc. p. 1-103.

Control Materials for Validating Measurement of Vitamin D in Key Foods for the USDA National Food and Nutrient Analysis Program (NFNAP) - (Abstract Only)

Holden, J.M., Byrdwell, W.C., Exler, J., Harnly, J.M., Holick, M., Hollis, B., Horst, R., Patterson, K.K., Phillips, K., Wolf, W.R. 2008. Control materials for validating measurement of vitamin D in key foods for the USDA National Food and Nutrient Analysis Program (NFNAP). Experimental Biology, April 5-9, 2008, San Diego, CA.

Spectral Fingerprints for Authentication and Identification of Variation in Foods and Botanical Materials - (Abstract Only)

Harnly, J.M., Luthria, D.L., Chen, P., Lin, L. 2008. Spectral Fingerprints for Authentication and Identification of Variation in Foods and Botanical Materials. Experimental Biololgy Meeting, April 5-9, 2008, San Diego, CA.

Chromatographic Profiles of Ginkgo biloba Leaves and Selected Products - (Abstract Only)

Lin, L., Chen, P., Ozcan, M., Harnly, J.M. 2008. Chromatographic Profiles of Ginkgo biloba Leaves and Selected Products. Experimental Biololgy Meeting, April 5-9, 2008, San Diego, CA.

Measuring Vitamins and Minerals in Dietary Supplements - (Abstract Only)

Dwyer, J., Piccian, M., Saldanha, L., Fisher, K., Yetley, E., Betz, J., Thomas, P., Coates, P., Holden, J.M., Andrews, K., Roseland, J.M., Zhao, C., Schweitzer, A., Harnly, J.M., Wolf, W.R., Perry, C., Milner, J., Whitted, J., Burt, V., Radimer, K., Wilger, J., Hardy, C., Sharpless, K. 2007. Measuring vitamins and minerals in dietary supplements. National Nutrient Databank Conference, April 27, 2007, Washington, DC.

Proposed minimum reporting standards for chemical analysis - (Peer Reviewed Journal)

Summer, L., Amberg, A., Barrett, D., Beale, M., Beger, R., Daykin, C., -M.Fan, T., Fiehn, O., Goodacre, R., Griffin, J., Hankemeir, T., Hardy, N., Harnly, J.M., Higashi, R., Kopka, J., Lane, A., Lindon, J., Marriott, P., Nicholls, A., Reily, M., Thaden, J., Viant, M. 2007. Proposed minimum reporting standards for chemical analysis. Metabolomics. 3:211-221.

Dietary Supplement Ingredient Database (DSID): Preliminary USDA studies on composition of adult multivitamin/mineral supplements - (Peer Reviewed Journal)

Roseland, J.M., Holden, J.M., Andrews, K., Zhao, L., Schweitzer, A., Harnly, J.M., Wolf, W.R., Perry, C., Dwyer, J., Picciano, M., Betz, J., Saldanha, L., Yetley, E., Fisher, K., Sharpless, K. 2007. Dietary Supplement Ingredient Database (DSID): Preliminary USDA studies on composition of adult multivitamin/mineral supplements. Journal of Food Composition and Analysis. 21(1): S69-S77. Available: doi:10.1016/j.fca.2007.07.009.

Measuring vitamins and minerals in dietary supplements for nutrition studies in the USA - (Peer Reviewed Journal)

Dwyer, J., Holden, J.M., Andrews, K., Roseland, J.M., Zhao, C., Schweitzer, A., Perry, C., Harnly, J.M., Wolf, W.R., Picciano, M., Fisher, K., Saldanha, L., Yetley, E., Betz, J., Coates, P., Milner, J., Whitted, J., Burt, V., Radimer, K., Wilger, J., Sharpless, K., Hardy, C. 2007. Measuring vitamins and minerals in dietary supplements for nutrition studies in the USA. Analytical and Bioanalytical Chemistry. 389(1):37-46.

Profiling Methods for the Determination of Phenolic Compounds in Foods and Dietary Supplements - (Peer Reviewed Journal)

Harnly, J.M., Bhagwat, S.A., Lin, L. 2007. Profiling methods for the determination of phenolic compounds in foods and dietary supplements. Analytical and Bioanalytical Chemistry. Available: doi:10.1007/s00216-007-1424-7.

Identification and quantification of flavanoids of Mexican oregano (Lippia graveolents) by LD-DAD-ESI/MS analysis. - (Peer Reviewed Journal)

Lin, L., Mukhopadhyay, S., Robbins, R.J., Harnly, J.M. 2007. Indentification and quantification of flavnoids of Mexican oregano (Lippia graveolents) by LD-DAD-ESI/MS analysis. Journal of Food Composition and Analysis, 20:361-369.

USDA's Composition Data for Fruits and Vegetables -- Sources, Measurement, and Variation - (Abstract Only)

Holden, J.M., Gebhardt, S.E., Haytowitz, D.B., Harnly, J.M. 2007. Usda's composition data for fruits and vegetables -- sources, measurement, and variation. Annual Conference of the American Society for Horticultural Science, July 16, 2007, Scottsdale, Arizona.

Chromatographic fingerprints analysis for evaluation of Ginkgo Biloba products - (Peer Reviewed Journal)

Chen, P., Ozcan, M., Harnly, J.M. 2007. Chromatographic Fingerprints Analysis for Evaluation of Ginkgo Biloba Products. Analytical and Bioanalytical Chemistry. Available on-line doi: 10.1007/s00216-007-1386-9.

Determination of the flavonoid components of cashew apple (Anacardium occidentale) by LC-DAD-ESI/MS - (Peer Reviewed Journal)

Sousa De Brito, E., Passanha De Araujo, M.C., Lin, L., Harnly, J.M. Determination of the flavonoid components of cashew apple (Anacardium occidentale) by LC-DAD-ESI/MS. Food Chemistry. 2007. Available http://dx.doi.org/ doi: 10.1016/j.foodchem.2007.02.009

Progress in Developing Dietary Supplement Databases: The Analytically Validated Dietary Supplement Ingredient Database (DSID) and Dietary Supplement Label Databases (DSLD) - (Peer Reviewed Journal)

Dwyer, J.T., Picciano, M., Betz, J.M., Fisher, K.D., Saldanha, L.G., Yetley, E.A., Coates, P.M., Milner, J., Whitted, J., Burt, V., Radimer, K., Wilger, J., Sharpless, K.E., Holden, J.M., Schweitzer, A., Andrews, K., Roseland, J.M., Zhao, C., Harnly, J.M., Wolf, W.R., Perry, C.R. 2007. Progress in developing dietary supplement databases: The analytically validated Dietary Supplement Ingredient Database (DSID) and Dietary Supplement Label Databases (DSLD). Journal of Food Composition and Analysis. Available: doi:10.1016/j.jfca.2007.07.010.

Flavonoids and Heart Health: Proceedings of the ILSI North American Flavonoids Workshop, May 13-June 1, 2005, Washington, DC - (Review Article)

Erdman, J., Balentine, D., Arab, L., Beecher, G., Dwyer, J., Folts, J., Harnly, J.M., Hollman, P., Keen, G.J., Messina, M., Messina, M., Scalbert, A., Vita, J., Williamson, G., Burrowes, J. 2007. Flavonoids and Heart Health. Journal of Nutrition. 137:718S-737S.

Detection and quantification of glycosylated flavonoid malonates in celery seed,(Apium graveolens L.)Chinese celery and celery by LC-DAD-ESI/MS - (Peer Reviewed Journal)

Lin, L., Lu, S., Harnly, J.M. 2007. Detection and quantification of glycosylated flavonoid malonates in celery seed,(Apium graveolens L.) Chinese celery and celery by LC-DAD-ESI/MS. Journal of Agricultural and Food Chemistry. 55:1321-1326.

FLAVONOID CONTENT OF U.S. FRUITS, VEGETABLES, AND NUTS. - (Peer Reviewed Journal)

Harnly, J.M., Doherty, R.F., Beecher, G.R., Holden, J.M., Haytowitz, D.B., Bhagwat, S.A., Gebhardt, S.E. 2006. Flavonoid content of U.S. fruits, vegetables, and nuts. Journal of Agricultural and Food Chemistry. 54:966-9977.

A Screening Method for the Identification of Glycosylated Flavonoids and Other Phenolic Compounds Using a Standard Analytical Approach for All Plant Materials - (Peer Reviewed Journal)

Lin, L., Harnly, J.M. A screening method for the identification of glycosylated flavonoids and other phenolic compounds using a standard analytical approach for all plant materials. Journal of Agricultural and Food Chemistry. 2007. 55:1084-1095.

The polyphenolic profiles of common bean (Phaseolus vulgaris L.) (Experimental Biology Annal Meeting, April, 2006, Washington, D.C) - (Abstract Only)

Lin, L., Harnly, J.M., Pastor Corrales, M.A., Luthria, D.L. 2007. The polyphenolic profiles of common bean (Phaseolus vulgaris L.). Experimental Biology, April 25, 2006, Washington, D.C.

Identification of the Phenolic Components of Arnica Flowers (Arnica montana L.) by LC-DAD-ESI/MS (Experimental Biology annual Meeting, April 2007, Washington, D.C.) - (Abstract Only)

Lin, L., Harnly, J.M. 2007. Identification of the Phenolic Components of Arnica Flowers (Arnica montana L.) by LC-DAD-ESI/MS. Experimental Biology, April 25, 2007, Washington, D.C.

"Food Composition" in Present Knowledge in Nutrition, Ninth Edition, Volume 1 - (Book / Chapter)

Holden, J.M., Harnly, J.M., Beecher, G. 2006. Food Composition. In: Bowman, B.A., Russell, R.M., editors. Present Knowledge in Nutrition, Ninth Edition, Volume 1. Washington, D.C.:International Life Sciences Institute. p. 781-794.

USDA DATABASE FOR THE FLAVONOID CONTENT OF SELECTED FOODS. RELEASE 2 - (Other)

Bhagwat, S.A., Gebhardt, S.E., Haytowitz, D.B., Holden, J.M., Harnly, J.M. 2006. Usda database for the flavonoid content of selected foods. release 2. USDA National Nutrient Database for Standard Reference.

USDA DIETARY SUPPLEMENT INGREDIENT DATABASE (DSID): ADULT MULTIVITAMIN/MINERAL STUDY - (Abstract Only)

Holden, J.M., Roseland, J.M., Andrews, K., Zhao, C., Schweitzer, A., Harnly, J.M., Wolf, W.R., Perry, C., Dwyer, J., Picciano, M., Saldanha, L., Betz, J. Usda dietary supplement ingredient database (dsid): adult multivitamin/mineral study. National Nutrient Databank Conference, September 18-20, 2006, Hawaii.

PREVALENCE OF VITAMINS E AND B12 IN DIETARY SUPPLEMENTS REPORTED IN NATIONAL HEALTH AND NUTRITION EVALUATION SURVEY (NHANES) - (Abstract Only)

Holden, J.M., Zhao, C., Roseland, J.M., Andrews, K., Amy, S., Perry, C., Wolf, W.R., Harnly, J.M., Dwyer, J., Picciano, M., Saldanha, L., Fisher, K., Betz, J., Yetley, E., Radimer, K., Wilger, J. Prevalence of vitamins e and b12 in dietary supplements reported in national health and nutrition evaluation survey (nhanes). Sixth International Conference on Dietary Assessment Methods, April 27-29, 2006, Copenhagen Denmark.

WHAT MORE DO WE NEED TO KNOW? RESEARCH UPDATE: THE DIETARY SUPPLEMENT INGREDIENT DATABASE: RESULTS OF USDA PILOT STUDIES - (Abstract Only)

Holden, J.M., Andrews, K., Roseland, J.M., Zhoa, C., Schweitzer, A., Wolf, W.R., Harnly, J.M., Perry, C., Dwyer, J., Saldanha, L., Picciano, M., Fisher, K., Yetley, E., Betz, J., Radimer, K., Bindewald, B., Sharpless, K. What more do we need to know? research update: the dietary supplement ingredient database: results of usda pilot studies. American Dietetic Association Annual Meeting: Food and Nutrition Conference and Expo, October 24, 2005, St. Louis, Missouri

IDENTIFICATION OF REPRESENTATIVE MULTIVITAMIN PRODUCTS IN THE UNITED STATES USING % DAILY VALUE LEVELS FOR HIGH PRIORITY NUTRIENTS - (Abstract Only)

Andrews, K., Zhao, C., Holden, J.M., Perry, C., Schweitzer, A., Roseland, J.M., Wolf, W.R., Harnly, J.M., Dwyer, J., Picciano, M., Saldanha, L. Identification of representative multivitamin products in the united states using % daily value levels for high priority nutrients. 6th International Food Data Conference - Food Composition Data and the Nutrition Dilemma, September 2005, Pretoria, South Africa.

PROGRESS IN DEVELOPMENT OF AN INTEGRATED DIETARY SUPPLEMENT INGREDIENT DATABASE AT THE NIH OFFICE OF DIETARY SUPPLEMENTS - (Peer Reviewed Journal)

Dwyer, J., Picciano, M., Betz, J., Leila, S., Holden, J.M., Andrews, K.W., Cuiwei, Z., Harnly, J.M., Wolf, W.R., Perry, C. 2006. Progress in development of an integrated dietary supplement ingredient database at the NIH Office of Dietary Supplements. Journal of Food Composition and Analysis. 19:S108-S114.

SELECTION OF REPRESENTATIVE MULTIVITAMIN PRODUCTS BASED ON % DAILY VALUE LEVELS FOR SPECIFIC NUTRIENTS - (Abstract Only)

Andrews, K., Zhao, C., Holden, J.M., Perry, C., Schweitzer, A., Wolf, W.R., Harnly, J.M., Dwyer, J., Picciano, M., Saldanha, L., Fisher, K., Betz, J., Yetley, E., Radimer, K., Bindewald, B. Selection of representative multivitamin products based on % daily value levels for specific nutrients. Experimental Biology Conference, April 2-6, 2005.

UPDATE OF USDA DATABASE FOR THE FLAVONOID CONTENT OF SELECTED FOODS - (Abstract Only)

Bhagwat, S.A., Haytowitz, D.B., Harnly, J.M., Holden, J.M. 2005. Update of usda database for the flavonoid content of selected foods. International Research Conference on Food, Nutrition and Cancer on July 14 & 15, 2005 at Hyatt Regency Washington on Capitol Hill, Washington, D.C.

USDA’S DATABASES FOR BIOACTIVE COMPOUNDS IN FOODS - (Abstract Only)

Holden, J.M., Bhagwat, S.A., Haytowitz, D.B., Gebhardt, S.E., Harnly, J.M. 2005. USDA’s databases for bioactive compounds in foods. Nutrition International Congress Proceedings, September 18-23, 2005, Durban, South Africa.

FREE AMINO ACID AND CYSTEINE SULFOXIDE COMPOSTION OF 11 GARLIC (ALLIUM SATIVUM L.) CULTIVARS BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION AND MASS SELECTIVE DETECTION - (Peer Reviewed Journal)

Lee, J., Harnly, J.M. 2005. Free amino acid and cysteine sulfoxide compostion of 11 garlic (allium sativum l.) cultivars by gas chromatography with flame ionization and mass selective detection. Journal of Agricultural and Food Chemistry. 53:9100-9104.

EFFECT OF SELENIUM FERTILIZER ON FREE AMINO ACID COMPOSITION OF BROCCOLI (BRASSICA OLERACEA CV. MAJESTIC) DETERMINED BY GAS CHROMATOGRAPHY WITH FLAME IONIZATION AND MASS SELECTIVE DETECTION - (Peer Reviewed Journal)

Lee, J., Finley, J.W., Harnly, J.M. 2005. Effect of selenium fertilizer on free amino acid composition of broccoli (brassica oleracea cv. majestic) determinded by gas chromatography with flame ionization and mass selective detection. Journal of Agricultural and Food Chemistry. 53:9105-9111.

SULFUR AND SELENIUM: NUTRIENTS, BIOACTIVE ELEMENTS, AND ANALYTICAL CHALLENGES - (Abstract Only)

Harnly, J.M., Rodriguez, L.E., Wolf, W.R. 2004. Sulfur and selenium: nutrients, bioactive elements, and analytical challenges. [abstract]. October: Paper No. P4.

A DISCUSSION ABOUT THE SIGNIFICANCE OF ABSORBANCE AND SAMPLE OPTICAL THICKNESS IN CONVENTIONAL ABSORPTION SPECTROMETRY AND WAVELENGTH MODULATED LASER ABSORPTION SPECTROMETRY - (Peer Reviewed Journal)

Harnly, J.M. 2004. A discussion about the significance of absorbance and sample optical thickness in conventional absorption spectrometry and wavelength modulated laser absorption spectrometry. Spectrochimica Acta, Part B. 59:389-392.

QUANTITATIVE DETERMINATION OF ALLICIN IN GARLIC: SUPERCRITICAL FLUID EXTRACTION AND STANDARD ADDITION OF ALLIIN - (Peer Reviewed Journal)

Rybak, M.E., Calver, E.M., Harnly, J.M. 2004. Quantitative determination of allicin in garlic: supercritical fluid extraction and standard addition of alliin. Journal of Agricultural and Food Chemistry. 52:682-687.

FOOD ENERGY - METHODS OF ANALYSIS AND CONVERSION FACTORS - (Monograph)

Maclean, W.C., Harnly, J.M., Chen, J., Chevassus-Agnes, S., Gilani, G., Livesey, G., Mathioudakis, B., Munoz De Chavez, M., Devasconcellos, M.T., Warwick, P. 2003. Food energy - methods of analysis and conversion factors. Food and Agriculture Organization of the United Nations Technical Workshop Report. Food and Nutrition Paper #77. ISSN 02543-4725, Rome, Italy.

FUTURE DIRECTIONS FOR WHAT WE EAT IN AMERICAN-NHANES: THE INTEGRATED CSFII-NHANES - (Peer Reviewed Journal)

Dwyer, J., Picciano, M., Raiten, D., Harnly, J.M., Holden, J.M., Wolf, W.R., Moshfegh, A., Pehrsson, P.R., Gebhardt, S.E., Ellwood, K.C. 2003. Future directions for what we eat in american-nhanes: the integrated csfii-nhanes. Journal of Nutrition. 133:624S-634S.

ORGANOSULFUR AND ORGANOSELENIUM COMPOUNDS: OCCURRENCE, IMPORTANCE, AND ANALYSIS - (Abstract Only)

Harnly, J.M. 2003. Organosulfur and organoselenium compounds: occurrence, importance, and analysis. [abstract]. Paper No. PO40.

THE SPATIAL DISTRIBUTION AND PHOTOMETRIC AND ANALYTICAL ACCURACY OF SN IN GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY IN THE PRESENCE OF SULFATES AND PALLADIUM - (Peer Reviewed Journal)

Ozcan, M., Akman, S., Schuetz, M., Murphy, J.R., Harnly, J.M. 2002. The spatial distribution and photometric and analytical accuracy of sn in graphite furnace atomic absorption spectrometry in the presence of sulfates and palladium. Journal of Analytical Atomic Spectrometry. 17:515-523.

EVALUATION OF PHOTOMETRIC ERRORS IN ABSORPTION MEASUREMENTS USING SPATIALLY RESOLVED CONTINUUM SOURCE GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY - (Peer Reviewed Journal)

Harnly, J.M., Schuetz, M., Murphy, J.R., Glmutdinov, A. 2001. Spatially resolved continuum source graphite furnace atomic absorption spectrometry. Journal of Analytical Atomic Spectrometry. 16:1241-1252

FOOD COMPOSITION - (Book / Chapter)

Holden, J.M., Harnly, J.M., Beecher, G.R. 2001. Food Composition. In: Bowman, B.A., Russell, R.M., editors. Present Knowledge in Nutrition. 8th Edition. Washington, DC: ILSI Press. p. 593-604.

CONTINUUM SOURCE-ATOMIC ABSORPTION SPECTROMETRY USING A TWO-DIMENSIONAL CHARGE COUPLED DEVICE - (Peer Reviewed Journal)

Schuetz, M., Murphy, J.R., Fields, R.E., Harnly, J.M. 2000. Continuum source-atomic absorption spectrometry using a two-dimensional charge coupled device. Spectrochimica Acta.

MULTIDIMENSIONAL INTEGRATION OF ABSORBANCES: AN APPROACH TO ABSOLUTE ANALYTE DETECTION - (Peer Reviewed Journal) - (20-Apr-99)

THE FUTURE OF ATOMIC ABSORPTION SPECTROMETRY: A CONTINUUM SOURCE WITH A CHARGE COUPLED ARRAY DETECTOR - (Peer Reviewed Journal)

Harnly, J.M. 1999. The future of atomic absorption spectrometry: a continuum source with a charge coupled array detector. Journal of Analytical Atomic Spectrometry. 14:137-146.

CHARACTERIZATION OF HYPERBOLIC CALIBRATION CURVES FOR CONTINUUM SOURCE ATOMIC ABSORPTION SPECTROMETRY WITH ARRAY DETECTION - (Peer Reviewed Journal) - (11-Sep-98)

SOLID STATE ARRAY DETECTORS FOR ANALYTICAL SPECTROMETRY - (Review Article) - (01-Sep-97)

USE OF A SEGMENTED ARRAY CCD DETECTOR FOR CONTINIUUM SOURCE ATOMIC ABSORPTION SPECTROMETRY WITH GRAPHITE FURNACE ATOMIZATIION - (Peer Reviewed Journal) - (14-Feb-97)

CHARACTERIZATION OF A MODIFIED TWO-STEP FURNACE FOR ATOMIC ABSORPTION SPECTROMETRY FOR SELECTIVE VOLATILIZATION OF FE SPECIES IN HEMIN - (Trade Journal) - (27-Aug-96)

INSTRUMENTATION FOR SIMULTANEOUS MULTIELEMENT ATOMIC ABSORPTION SPECTROMETRY WITH GRAPHITE FURNACE ATOMIZATION - (Peer Reviewed Journal) - (09-Feb-96)

EXTENDED CALIBRATION RANGES FOR CONTINUUM SOURCE ATOMIC ABSORPTION SPECTROMETRY WITH ARRAY DETECTION - (Peer Reviewed Journal) - (30-Nov-95)